崔丽, 武德凡, 杨泽卿, 贺定勇, 吴旭, 曾勇, 曹庆. 热处理对SLM成形TC4合金组织及性能的影响[J]. 北京工业大学学报, 2023, 49(9): 970-979. DOI: 10.11936/bjutxb2022050014
    引用本文: 崔丽, 武德凡, 杨泽卿, 贺定勇, 吴旭, 曾勇, 曹庆. 热处理对SLM成形TC4合金组织及性能的影响[J]. 北京工业大学学报, 2023, 49(9): 970-979. DOI: 10.11936/bjutxb2022050014
    CUI Li, WU Defan, YANG Zeqing, HE Dingyong, WU Xu, ZENG Yong, CAO Qing. Effect of Heat Treatment on Microstructure and Properties of TC4 Alloys Fabricated by Selective Laser Melting[J]. Journal of Beijing University of Technology, 2023, 49(9): 970-979. DOI: 10.11936/bjutxb2022050014
    Citation: CUI Li, WU Defan, YANG Zeqing, HE Dingyong, WU Xu, ZENG Yong, CAO Qing. Effect of Heat Treatment on Microstructure and Properties of TC4 Alloys Fabricated by Selective Laser Melting[J]. Journal of Beijing University of Technology, 2023, 49(9): 970-979. DOI: 10.11936/bjutxb2022050014

    热处理对SLM成形TC4合金组织及性能的影响

    Effect of Heat Treatment on Microstructure and Properties of TC4 Alloys Fabricated by Selective Laser Melting

    • 摘要: 选区激光熔化(selective laser melting, SLM)成形TC4合金组织因极快的冷却速度形成了大量硬脆的针状α'马氏体, 导致SLM成形TC4合金塑性显著降低, 严重限制了SLM成形TC4合金的工程应用。为了提高SLM成形TC4合金的塑性, 研究了4种不同热处理温度对SLM成形TC4合金微观组织及力学性能的影响。结果表明, 4种不同温度热处理后, 初生β晶粒内的针状α'相转变为α相, 且随着温度从860 ℃增加到950 ℃, 针状α相形态从网篮状转变为相同取向的集束, α晶粒尺寸从1.73 μm增大到2.32 μm, β相体积分数从0.4%增大到2.7%。抗拉强度从961 MPa降低到870 MPa, 而延伸率则先升高后降低, 其中890 ℃热处理的抗拉强度为941 MPa, 延伸率为11.1%, 相对于未热处理试样, 延伸率提高了126.5%。

       

      Abstract: A large number of hard and brittle needle-like α' phases are presented in the microstructure of TC4 alloys fabricated by selective laser melting (SLM) due to the extremely fast cooling rates, resulting in a significant decrease in the plasticity of SLM TC4 alloys, which seriously limits their engineering applications. To improve the plasticity of the SLM TC4 alloys, the effect of different heat treatment temperatures on microstructure and mechanical properties of SLM TC4 alloys was systematically investigated. Results show that the needle-like α' phase in the primary β grains is transformed into the α phase after heat treatments at four temperatures. With the heat treatment temperature increasing from 860 ℃ to 950 ℃, the morphology of the needle-like α phases is transformed from basket-like distribution into a colony with the same orientation. Furthermore, the grain size of α phases increases from 1.73 μm to 2.32 μm and the fraction of β phases increases from 0.4% to 2.7%. The ultimate tensile strength (UTS) of SLM TC4 alloys is slightly reduced from 961 MPa to 870 MPa while the elongation index (EI) of the SLM TC4 alloys first increases and then is reduced. Among the temperatures, the UTS of 941 MPa and the EI of 11.1% are obtained by heat treatment at 890 ℃, which increases by 126.5% compared with the unheat-treated samples.

       

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